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Batch Products Atlas Calorimeter
Atlas Calorimeter - Syrris - High Performance Reaction Calorimeter
Atlas Reaction Calorimeter
The Atlas Calorimeter is an easy-to-use, high performance system. Using either Heat Flow Calorimetry (HFC) or Power Compensation Calorimetry (PCC), Atlas can generate power and enthalpy graphs quickly and easily.
This, combined with the simple configuration of reaction temperatures, dosing quantities and alarms provides chemistry laboratories with an easy, safe and accurate calorimetry system. Based on the standard Atlas Potassium, the Atlas Calorimeter also includes a power supply and the intelligent Atlas Software that can create graphs within seconds.
For more information on the Atlas Calorimeter, please watch the video below. For those without sound, English subtitles are included by default.
Benefits and Specifications:
- Fully automated: Temperature control, set up and operation are all automated.
- Excellent control: Sophisticated PID control and powerful circulators result in accurate isothermal performance.
- Accurate: Vacuum jacketed vessels, automated calibration and sensitive RTDs give extremely high accuracy results.
- Walk away operation: Automated gravimetric or volumetric reagents additions are all made easy.
- High performance overhead stirrer: Improved formulation consistency, stability and performance of final drug products.
- Easy analysis: Easy to use software allows graphs of power and enthalpy to be plotted with one click.
- Quick: Everything clicks together quickly and easily without the need for tools. Vessels can be changed in under 1 minute.
- Flexible: The same equipment and software can be used for HFC or PCC, allowing the chemist to pick the best method for the reaction.
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More Info
Atlas HFC and PCC System features
Atlas PC Software offers truly easy calorimetry operation. Configuration of parameters such as reaction temperature, dosing quantities, expected power level (e.g. moderate endotherm; strong exotherm) and alarms (with subsequent actions) are defined in an easy to use wizard.
When running the experiment, everything is controlled automatically including stabilization at desired reaction temperature, reagent addition and in the case of HFC, pre and/or post run calibration. No user intervention is required during the entire process. All data is continually logged to a common csv file and displayed by the software in graph format in real time.
The software automatically includes the calibration, compensates for the enthalpy of addition and deviations from isothermal conditions. Analysis is made easy by the Atlas Software featuring “single click” plotting of power and enthalpy.
Specification and Parts
Specification
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Interchangeable Jacketed Reaction Vessels: |
100ml, 250ml, 500ml, 1 litre and 2 litre vacuum jacketed reactors available with a range of profiles including round, torispherical, conical or custom. |
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Temperature Range: |
-40°C to 150°C recommended for calorimetry (up to 200°C possible). |
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Accuracy: |
Typically 1 to 5% (dependent on settling time and external conditions). |
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Calorimetric Techniques Used: |
Heat flow calorimetry (HFC) or power compensation calorimetry (PCC). |
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Footprint: |
From 40cm (16”) wide. |
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Chemical Resistance: |
Glass, PTFE and other fluoropolymers. |
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Maximum Reaction Power: |
100W/litre maximum (50W for power compensation calorimetry). |
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Safety Features: |
Warnings, alarms and automatic shutdown can be set for the whole experiment and each process step. |
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Stirring Options: |
Anchor, pitched blade propeller, retreat curve impeller or custom made in glass or PTFE. 0-800RPM (up to 11Ncm) or 0-1000RPM (up to 90Ncm) with torque feedback. |
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Circulator Options: |
Julabo, Huber, Lauda, Haake |
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Equipment Supplied: |
Standard Atlas Potassium System, plus: |
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Atlas PC Software |
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Atlas Calorimetry Software Upgrade and Atlas Reporting Software |
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Atlas Port for recirculator control |
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Vacuum jacketed vessel (see above) |
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Fast response reaction temperature probe |
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Tj (jacket in) measurement probe with node and insulated cover |
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PC controlled heater power supply with Atlas Port |
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Reactor heater |
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Dosing Options: |
Manual dosing, Atlas Syringe Pump for automatic volumetric dosing or peristaltic pump and balance for gravimetric dosing. |
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Other Sensor Options: |
pH, in-situ FTIR sensor, turbidity, pressure, etc. |
Parts list
| Description | Part Number |
| Atlas Potassium (minus regular RTD Probe) |
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| Atlas Software 1 |
2300102 |
| Atlas Calorimetry Software Upgrade |
2600003 |
| Atlas Reporting Software | 2600002 |
| TTI Power Supply for Calorimetry (230V) / (115/V) | 2200141 / 2200151 |
| Heater Rod | See the Syrris Batch Chemistry Reactors 2012 Catalogue |
| Temperature Probe | 2101021 |
| Quick Response RTD Probe | See the Syrris Batch Chemistry Reactors 2012 Catalogue |
| RTD - Stainless Steel 100mm x 3mm | 2101593 |
| Vacuum Jacketed Vessel | See the Syrris Batch Chemistry Reactors 2012 Catalogue |
| Velcro Oil Connector Insulator (Pack of 2) | 2200008 |
| Option | |
| Atlas Syringe Pump | 2200072 |
Related docs
Downloads
- Click here to download the Atlas Calorimeter Brochure
- Click here to download the Atlas Brochure
- Click here to download the Syrris Batch Chemistry Reactors 2012 Catalogue
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