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Batch Products Atlas Jacketed Reactors Atlas FT-IR Spectrometer
Atlas FT-IR Spectrometer - Syrris - Infrared Reaction Monitoring
Atlas FT-IR Spectrometer
The Atlas FT-IR System is a high performance, automated laboratory reactor with an integrated mid-IR spectrometer. The combination of the Syrris Atlas and Bruker Optics Matrix-MF makes it ideal for real-time analysis of chemical reactions and processes.
- Real time, in situ, quantitative analysis: Can be used for analysing product yield, impurities, reaction kinetics, mechanism, end point, etc.
- Easy to upgrade: Calorimetry, pH control, gravimetric or volumetric reagent addition, crystallizations, parallel reactions, etc.
- Wide temperature and pressure range: -80°C to +180°C and vacuum to 300bar† (†with custom reactors).
- Fully automated with integrated analysis: Fully automated reactor control. IR data from the Matrix-MF can be displayed alongside other process data in the Atlas Software.
- Wide range of vessel sizes: 50ml, 100ml, 250ml, 500ml, 1L, 2L, 3L* and 5L* (*with remote mount).
- Quick change vessel: The oil drain unit, jacketed vessel clamp, auto aligning stirrer and quick oil connectors allow vessels to be changed in under a minute.
- Wide wave number range: Analysis is possible from 3,500 to 560cm-1.
- Easy to use: Twist and click knob, large display and intuitive “drag and drop” software.
- Robust: An extremely chemically resistant reactor system and FTIR probe with vibration resistant optics.
- Compact: The Atlas footprint of 23cm (9”) square and Matrix-MF footprint of 30cm (12”) square easily fits into fume cupboards.
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Atlas FT-IR System software features
The Bruker Optics Matrix-MF OPUS software is integrated with the Syrris Atlas Software to make it easy to control and to view results. Data such as integrated peak size (over a defined wavenumber range) can be plotted on the same graph as other Atlas data e.g. reaction power, enthalpy, pH, temperature and user added comments.
A waterfall plot from the Bruker Optics Matrix-MF OPUS software
Specification and Parts
Specification
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Working Volume Options: |
50ml, 100ml, 250ml, 500ml, 1 litre, 2 litres, 3 litres or 5 litres (vessels are interchangeable). Note that vessels greater than 2 litres also require the Remote Mount. |
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Reaction Vessel Profile Options: |
Round bottom, torispherical or conical. Custom available on request. |
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Stirrer Options: |
Anchor, pitched blade propeller, retreat curve (in glass or PTFE), custom available on request. |
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Chemical Resistance: |
All wetted parts made from glass and PTFE (or other similar fluoropolymers) |
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Maximum Temperature: |
+200°C (+250°C with High Temperature Upgrade Kit). The maximum temperature achievable is also circulator dependent. |
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Minimum Temperature: |
-80°C. The minimum temperature achievable is also circulator dependent. |
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Temperature Accuracy: |
Class A RTDs, displayed to 3 decimal places. PID temperature control of process temperature. |
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Pressure: |
Vacuum (50mbar) to 0.5 bar (see Atlas Pressure Systems for high pressure). |
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Overhead Stirring: |
Scorpion Overhead Stirrer to 800RPM with 11Ncm Torque (High torque options available to 180Ncm peak, 90Ncm continuous with speed of 1000RPM and torque feedback). |
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Modes of Operation: |
Manual (set on Atlas Base), Automated (set on Atlas Base) or full PC Software control. |
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Source: |
MID-IR. |
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Spectal Range: |
3,500 - 560cm-1. |
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Fiber Optical Cable: |
Silver halides (1mm dia). |
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Beam Splitter: |
KBr. |
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IR Transmission: |
Approx. 1% at finger print region. |
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MCT Detector: |
Liquid N2 cooled (optional |
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Probe: |
Diamond ATR probe |
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Temperature: |
-80°C to +180°C |
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Probe Head Length: |
290mm +/-20mm |
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Probe Head Diameter: |
6mm |
Parts list
| Description | Part Number |
| Atlas Potassium |
|
| Bruker FT-IR Spectrophometer Marix MF |
RD2200249 |
| Bruker Atlas Software Drivers |
RD2600005 |
Related docs
Downloads
- Click here to download the Atlas FT-IR System Flyer
- Click here to download the Atlas Brochure
- Click here to download the Syrris Batch Chemistry Reactors 2012 Catalogue
Video