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Batch Products Atlas Pressure Reactors Atlas Potassium Pressure
Atlas Potassium Pressure - Syrris - 3 Bar Jacketed Reactor
Atlas Potassium Pressure
The Atlas Potassium Pressure System is a modular 3 bar pressure reactor system that can be controlled automatically or manually. It is available with reactors in volumes of 100ml, 250ml, 500ml, 1L, 2L or 3L to 3 litres (all with or without vacuum jacket) that can be changed in under a minute without the need for tools.
The Atlas Potassium Pressure System is designed for applications where elevated pressures are required e.g. hydrogenations, carbonylations etc. or high vacuum applications. The basic system allows automatic temperature control (-80°C to +200°C) and stirrer control (up to 800RPM or 2000RPM) and pressure sensing. This data is also displayed and automatically logged by the base. The system includes a burst disc, pressure relief valve and complies with PED / ASME design codes.
Upgrades include the Gas Selection Module, Pressure Control Module, gas flow meters/controllers and full PC software control and automation. For more information, please contact Syrris.
Benefits
- Quick change vessel: The oil drain unit, jacketed vessel clamp and quick oil connectors allow vessels to be changed in under a minute.
- Easy to use: No tools required, twist and click control knob, large display and intuitive.
- High performance stirring: The Atlas Potassium Pressure System offers powerful overhead stirring.
- 3 bar pressure: The Atlas Potassium Pressure System has an operating pressure of up to 3 bar (see the Custom Reactor Systems for higher pressure).
- Variety of vessels: The Atlas Potassium Pressure System can be supplied with 100ml, 250ml, 500ml, 1L, 2L or 3L glass reaction vessels with or without vacuum jacket.
- Safe: Burst disc, pressure relief valve and complies with PED / ASME design codes.
- Automation and data-logging without PC: Automatic profiles are possible for reaction temperature, stirrer speed, reagent addition and sampling. All data is logged in a .csv file and can be downloaded to a USB stick automatically.
- Optional PC control: The PC software offers advanced recipe control, total automation of all parameters, alarms and real time graphs.
- Wide temperature range: -80 to +200°C.
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Atlas Potassium Pressure System features
The Atlas Potassium Pressure System is designed for applications where elevated pressures are required e.g. hydrogenations, carbonylations, etc.
The basic system, allows automatic temperature and stirrer control and pressure sensing. Upgrades include the Gas Selection Module, Pressure Control Module, gas flow meters and full PC software control and automation. For more information, please contact Syrris.
Modes of operation
Manual Pressure Control
Use the Atlas Pressure Node and Sensor with manual valves to control pressure. Pressure, temperature and stirrer speed are displayed and logged automatically.
Automatically Maintain a Pressure
By using the Atlas Pressure Control Module a consistent pressure to the reaction is maintained over the reaction period and can automatically vent in the case of over pressure. This module also offers, Vent and Purge options.
Pressure Control with Mass Flow Monitoring
Maintain a pressure and monitor mass flow. Ideal for gas uptake monitoring.
Mass Flow Control
Dose a known quantity of gas using the mass flow controller.
Off Gas Monitoring
Monitor off-gases with mass flow meters.
*Manual or Automated Gas Selection
All of the above modes of operation are available with the Atlas Gas Selection Module, allowing manual or automated selection of up to 3 gases.
Specification and Parts
Specification
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Working Volume Options: |
100ml, 250ml, 500ml, 1 litre, 2 litres or 3 litres (vessels are interchangeable and available with or without vacuum jacket). Note that larger vessels also require the Remote Mount. |
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Reaction Vessel Profile Options: |
Round bottom. Custom available on request. |
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Stirrer Options: |
Anchor, pitched blade propeller, retreat curve (in glass or PTFE), custom available on request. |
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Chemical Resistance: |
All wetted parts made from glass and PTFE (or other similar fluoropolymers) |
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Maximum Temperature: |
+200°C. The maximum temperature achievable is also circulator dependent. |
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Minimum Temperature: |
-80°C. The minimum temperature achievable is also circulator dependent. |
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Temperature Accuracy: |
Class A RTDs, displayed to 3 decimal places. PID temperature control of process temperature. |
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Pressure: |
Vacuum (50mbar) to 3 bar (see Custom Reactor Systems for high pressure). |
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Overhead Stirring: |
Scorpion Overhead Stirrer to 800RPM with 11Ncm Torque (High torque options available to 180Ncm peak, 90Ncm continuous with speed of 1000RPM and torque feedback). |
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Levels of Automation: |
Manual (set on Atlas Base), Automated (set on Atlas Base) or full PC Software control. |
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Safety: |
Burst disc and pressure relief valve. |
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Upgrade options include: |
Reaction calorimetry, automated liquid dosing, FTIR analysis, reaction sampling, pH analysis and control etc. |
Parts List
| Description | Part Number |
| Base unit | 2101000 |
| Scorpion Overhead Stirrer | 2101004 |
| Temperature Node | 2101021 |
| Pressure Sensor | 2200370 |
| Pressure Node | 2200369 |
| 2 x Node Extensions | 2101023 |
| Triple Node Socket | 2101024 |
| Stirrer Seal and Guide (3 Bar System) Stainless Steel/PTFE | 2200334/2200405 |
| Jacketed Vessel Clamp (3 Bar System) | 2200333 |
| Oil Drain Unit | 2101013 |
| Jacketed Vessel (Rated to 3 bar) | Various |
| Jacketed Vessel Lid and Safety Manifold (3 Bar System) | 2200335 |
| 6/8/9mm Probe Holder (3 Bar System) | 2200426/7/8 |
| Oil Pipes from Reactor to Oil Drain Unit (Pack of 2) | 2101014 |
| Reaction Vessel Drip Tray | 2101039 |
| Support Rods (Pack of 2) | 2101009 |
| Stirrer | Various |
| RTD Probe | Various |
| Base to Circulator Serial Cable (RJ11 to DB9 Male) | 2400214 |
| Reaction Vessel Seal (FFKM) | 2101543 |
| 3 Bar System Starter Kit (Selection of Pipes and Fittings) | 2200409 |
| Safety Cabinet for 3 Bar System | RD2200474 |
| Options | |
| Gas Selection Module | 2200375 |
| Gas Pressure Control Module | 2200388 |
Related Docs
Downloads
- Click here to download the Atlas Brochure
- Click here to download the Syrris Batch Chemistry Reactors 2012 Catalogue
Video