Atlas Sodium Pressure - Syrris - Automate Reactions up to 200 bar

Atlas Sodium Pressure

Atlas Sodium Pressure Logo

The Atlas Sodium Pressure System is designed for applications where elevated pressures (up to 200bar) or temperatures (up to 320ºC) are required e.g. hydrogenations, carbonylations, etc. It is a modular pressure reactor system that can be controlled automatically or manually. Available in volumes of 100, 160, 300 and 450ml in stainless steel 316, hastelloy, titanium, etc., the Atlas Sodium Pressure System offers heating and/or cooling, overhead stirring (to 800RPM) or magnetic stirring (to 1200RPM).

The reactor, shown opposite, includes a dip tube for sampling, a cooling coil, a thermowell, an impellor, valves, a manual pressure gauge and burst disc. It complies with PED / ASME design codes.

The basic system allows automatic temperature and stirrer control and pressure sensing. Upgrades include the pressure node and sensor for pressure logging, Gas Selection Module, Pressure Control Module, gas flow meters and full PC software control and automation. For more information, please contact Syrris.

Benefits

High pressure: The Atlas Sodium Pressure System has an operating pressure of up to 200 bar (contact Syrris for higher pressures).
Easy to use: Dry Bath for high pressure reactor is designed to fit easily and safely on the Atlas hotplate.
Advanced control: The PC software offers gas selection and automated pressure or mass flow control.
High performance stirring: The Atlas Sodium Pressure System offers powerful overhead (up to 800RPM) or magnetic stirring (up to 1200RPM).
High operating temperature: Will operate to temperatures up to 250°C (contact Syrris for higher temperatures).
Versatile: The Atlas Sodium Pressure System offers liquid sampling at high pressures/temperatures.
Ideal for catalyst screening: Quick automation and optimisation of high pressure reactions.
Variety of vessels: The Atlas Sodium Pressure System can be supplied with 100, 160, 300 and 450ml reaction vessels in stainless steel 316, hastelloy, titanium, etc.
Safe: Burst disc, maximum temperature cut out and complies with PED / ASME design codes.
Data-logging without PC Software: All data such as pressure, temperature, stirrer speed, etc. is logged automatically.

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Atlas Sodium Pressure System features

The Atlas Sodium Pressure System is designed for applications where elevated pressures (up to 200bar) or temperatures (up to 320ºC) are required e.g. hydrogenations, carbonylations, etc.

Modes of operation

Manual Pressure Control

Use the Atlas Pressure Node and Sensor with manual valves to control pressure. Pressure, temperature and stirrer speed are displayed and logged automatically.

Automatically Maintain a Pressure

By using the Atlas Pressure Control Module and the PC software a consistent pressure to the reaction is maintained over the reaction period.

Pressure Control with Mass Flow Monitoring

Maintain a pressure and monitor mass flow. Ideal for gas uptake monitoring.

Mass Flow Control

Dose a known quantity of gas using the mass flow controller.

Off Gas Monitoring

Monitor off-gases with mass flow meters.

*Manual or Automated Gas Selection

All of the above modes of operation are available with the Atlas Gas Selection Module, allowing manual or automated selection of up to 3 gases.

Specification and Parts

Specification

Safety:	Burst disc.
Working Volume Options:	100ml, 160ml, 300ml or 450ml.
Stirrer:	Pitched blade propeller. Custom available on request.
Chemical Resistance:	All wetted parts are made from Stainless Steel 316 (Hastelloy also available).
Maximum Temperature:	+280°C hotplate temperature (350°C hotplate temperature with hotter hotplate).
Minimum Temperature:	Room temperature (-40°C cold plate temperature with Hot and Cold Plate).
Temperature Accuracy:	Class A RTDs, displayed to 3 decimal places. PID temperature control of process temperature.
Pressure:	Vacuum (50mbar) to 200 bar (see Atlas Pressure Systems for high pressure).
Overhead Stirring:	Scorpion Overhead Stirrer to 800RPM with 11 Ncm torque (high torque options available to 180 Ncm peak, 90 Ncm continuous with speed of 1000RPM and torque feedback.
Modes of Operation:	Manual (set on Atlas Base), automated (set on Atlas Base) or full PC software.
Liquid Sampling:	Possible using valve and dip tube.

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If you would like more information about the Atlas Sodium Pressure System, Atlas Potassium Pressure System or any of the products in the Atlas range, click here to contact us