Pre-configured System

Atlas Potassium Pressure Reactor: 3 Bar Pressure Vessel

A modular 3 bar pressure reactor system that can be controlled automatically or manually.  Available with reactor volumes from 100 mL to 3 L that can be changed in minutes without the need for tools.

Atlas high pressure reactor at a glance

The Atlas Potassium 3 Bar Reactor is designed for chemical processes that require a wide range of operating pressures, such as hydrogenations, carbonylations, or high-vacuum applications.

The basic system allows automatic temperature control from -80 °C to +200 °C, stirrer control of up to 800 RPM or 2000 RPM, and pressure sensing.

  • Reactor volumes from 100 mL to 3 L
  • Automatic temperature control (-80 °C to +200 °C)
  • Stirrer control (up to 800 RPM or 2000 RPM)

Meet The Atlas HD Families

  • Reactor volumes from 100 mL to 3 L
  • Automatic temperature control (-80 °C to +200 °C)
  • Stirrer control (up to 800 RPM or 2000 RPM)

1. Powerful control

The high pressure reactor can be controlled using the Atlas base or the Atlas PC Software, providing a graphical display of pressures, temperatures, etc. Mass flow meters and controllers can also be integrated.

A Chemist using the gas module of Atlas HD 3 Bar Pressure System
A chemist using Syrris Atlas HD's touchscreen
A chemist using Syrris Atlas' automation software

2. Wide Vessel Range with Seamless Interchangeability

Seamlessly drain the oil from your jacketed reactor using the Oil Drain Unit and change reactors in minutes.  The system has a wide range of vessels, all rated to 3 bar, including 100 mL, 250 mL, 500 mL, 1 L, 2 L or 3 L, with or without a vacuum jacket.  The tool-free vessel clamp supports the reactors to ensure safe vessel change without any fuss or spillages.

 

Syrris Atlas HD 3 Bar Pressure System assembly
Loading a vessel into Atlas HD

3. Safe and convenient

The Atlas Potassium 3 bar system combines all the great user features of Atlas with all the safety features you would expect from a pressure system. It is equipped with a factory-set maximum pressure burst disc and pressure relief valve to ensure the glass reactor can never see an unexpected pressure rise.  The safety enclosure has been designed to provide that extra peace of mind and to ensure a very safe laboratory.

A chemist opening up the safety enclosure of Syrris Atlas HD 3 Bar Pressure System
Syrris Atlas HD 3 Bar Pressure System, in the lab

4. Precise temperature control

The system has a wide temperature range from -80 to +200 °C with accurate thermal control using either the touchscreen base or PC control software.  Simply connect a compatible circulator to the base unit or PC software and precision temperature algorithms will ensure your process performs without issues.

Syrris Atlas HD Ice on a vessel

5. Easy to use

Consistent with all the systems in the Atlas range, no tools are required, allowing simple twist-and-click configuration of the apparatus, large displays and intuitive control from the base unit or PC software.

Additionally, integrated filters can be used to separate solid catalysts from the mixture, enhancing the efficiency and purity of processes.

6. Stirred Autoclave Functionality

The system is equipped with an optimizedirrer that ensures thorough mixing of reactants, promoting uniform reaction conditions and improving efficiency and yield. Made from high quality materials, the pressure vessel is designed to withstand corrosive environments and maintain integrity under high pressures.

Safety features such as a factory-set maximum pressure burst disc, pressure relief valves, and a robust sealing system prevent leaks and ensure safe operation under elevated pressures. The stirred autoclave can be easily integrated with other modules and accessories, allowing for customized setups tailored to specific research needs.

 

What our customers say

We run two Atlas 3 Bar reactor systems in parallel, and can quickly and easily configure the reactors for advanced applications such as calorimetry and crystallization control”

Supabhorn Khaubunsongserm, Researcher, Process Technology Research Department, PTT
A hand drawn sketch of Syrris Atlas HD by Scott Clunas, Process Chemist, TauRx Therapeutics, Aberdeen, UK

Specifications

Vessel Volume Range 50 mL, 100 mL, 250 mL, 500 mL, 1 L, 2 L (DN80), 1 L, 2 L, and 5 L (DN150)
Vessel Shapes Torispherical, Conical, Round Bottom
Vessel Profiles Jacketed, Vacuum Jacketed
Other Vessel Types No (Round bottomed flasks can be used with the Atlas Classic base, but not with the 3 bar pressure system)
Temperature Range -90°C to 250°C (with suitable seal kit)
Stirring Options Scorpion Overhead Stirrer (up to 800rpm/11Ncm torque), High Speed Available, High Torque Available
Automation Yes – as standard
Modes of Operation Atlas PC Software, Manual Operation, AtlasClassic Click Wheel Control
Sensor Options Temperature, pH, Pressure, Turbidity, In-situ FTIR, Other Sensors Available
Pressure Range Vacuum (50mbar) to 3 Bar, See Atlas 200 Bar Pressure Systems for High Pressure up to 200 Bar
Reaction Calorimetry Ability to Upgrade to Reaction Calorimetry, See Atlas HD Calorimeter
Reagent Addition and Sampling Manual Dosing, Automated Dosing (Volumetric), Automated Dosing (Gravimetric), Sampling of Liquids, Full Gas Control, Atlas Syringe Pump Range

More Atlas HD Modules

Syrris Atlas HD 3 Bar Pressure System, Safety Enclosure close-up
Syrris Atlas HD Base Unit
Syrris Atlas HD 3 Bar Pressure System, close-up of pressure dial
Atlas HD Texture - scorpion overhead stirrer motor

Laboratory applications: High-pressure reactor uses

The Atlas Potassium 3 Bar System is designed to excel in a variety of pressurized laboratory applications, offering reliable performance for both lab. Its robust construction and advanced features make it ideal for:

Hydrogenations

Utilize the system’s pressure vessel capabilities to efficiently add hydrogen to organic compounds. The stainless steel construction ensures resistance to corrosion, maintaining the purity of reactions.

Carbonylations

The Atlas 3 Bar System supports carbonylation by facilitating the introduction of carbon monoxide into organic compounds under controlled pressure conditions. This is crucial for synthesizing aldehydes, ketones, and carboxylic acids.

Reactions under a range of pressure

This system is suitable for high-vacuum conditions. The inert inner surfaces prevent contamination, providing a clean reaction environment.

Corrosion testing

The system’s robust glass pressure vessel is perfect for testing the corrosion resistance of materials under high-pressure conditions, ensuring the long-term durability and reliability of products.

Homogeneous and heterogeneous catalysis

The advanced control systems and modular design of the Atlas 3 Bar System support both homogeneous and heterogeneous catalysis, providing precise control over conditions.

Polymerization Reactions

The system can be used for polymerization reactions, which requires elevated pressures to ensure uniform polymer formation and enhanced material properties.

Hydrothermal Synthesis

Ideal for synthesizing advanced materials like zeolites and metal-organic frameworks under high-pressure and high-temperature conditions.

Modules

  1. Base units

    • Atlas Classic Base

      (included)

      The Base Unit is the centre of any Atlas system. The Base Unit can be configured into a variety of different systems for different applications such as discovery or process chemistry. In every case, the hardware clicks into place in seconds without the need for tools.

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  2. Vessels and Stirrers

    • Atlas Scorpion Overhead Stirrer

      (included)

      The Atlas Scorpion Overhead Stirrer is a quick release, high RPM stirrer motor, and coupling. The Scorpion Overhead Stirrer provides […]

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    • Stirrer Seal and Guide (Atlas 3 bar System)

      (included)

      The Stirrer Seal and Guide is rated to 3 bar and is designed for use with the Atlas 3 Bar […]

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    • Jacketed Vessels (rated to 3 bar)

      (included)

      There is a range of jacketed reactor vessels that are rated to 3 bar and are designed for use with […]

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    • Vessel Lid and Safety Manifold (3 bar system)

      (included)

      The Jacketed Vessel Lid and Safety Manifold for the 3 bar system is designed for use with the Jacketed Vessel […]

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  3. Probes and Nodes

    • Temperature Node and Probe

      (included)

      Easy connection to the Atlas HD base. Our probes are available in different lengths to suit different vessels.

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    • Pressure Sensor and Nodes (Atlas 200 Bar Pressure System)

      (included)

      Sensor for sensing pressure in the reactor and node to couple to Atlas base. Pressure Sensor for 200 Bar System […]

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  4. Automation

    • Atlas PC Software 1

      (optional)

      Atlas Software 1 is an easy-to-use PC based application for control and analysis of experiments. Whole systems including stirrers, circulators, […]

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  5. Advanced Applications

    • Atlas Jacketed Vessel Clamp (3 Bar System)

      (included)

      The Jacketed Vessel Clamp for the 3 bar system is designed to accept any of the Syrris Jacketed Vessel (rated […]

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    • Atlas Safety Enclosure (3 bar)

      (included)

      The safety enclosures for the Atlas 3 Bar Pressure System offers a compact and safe shield when pressurizing vessels and […]

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    • Atlas Gas Selection Module

      (optional)

      The Gas Selection Module allows 3 gases to be permanently connected to the module yet only one gas connected to […]

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    • Atlas 200 Bar Gas Pressure Control Module

      (optional)

      This module automatically controls the dosing of gas into and out of the reactor to control the pressure within the […]

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    • Aalborg Mass Flow Controllers

      (optional)

      The Aalborg Mass Flow Controller is for use with Atlas Pressure Systems. It is ideal for applications such as dosing […]

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    • Aalborg Mass Flow Meter

      (optional)

      The Aalborg Mass Flow Meters are for use with Atlas Pressure Systems. They are ideal for applications such as understanding […]

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  6. Circulation

    • Atlas Oil Drain Unit, Oil Pipe Tidy, and Oil Pipes

      (included)

      The perfect accessory for those wishing to change vessels with as little fuss and mess as possible. Atlas HD Oil […]

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    • Circulator and Fluid

      (optional)

      Circulator options from industry-leading manufacturer, Huber. A range of circulator accessories and oils for whatever your application are available.

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  7. Dosing

  8. Optional modules

    • Atlas Gas Selection Module

      (optional)

      The Gas Selection Module allows 3 gases to be permanently connected to the module yet only one gas connected to […]

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    • Atlas 200 Bar Gas Pressure Control Module

      (optional)

      This module automatically controls the dosing of gas into and out of the reactor to control the pressure within the […]

      View module details
    • Atlas PC Software 1

      (optional)

      Atlas Software 1 is an easy-to-use PC based application for control and analysis of experiments. Whole systems including stirrers, circulators, […]

      View module details
    • Aalborg Mass Flow Controllers

      (optional)

      The Aalborg Mass Flow Controller is for use with Atlas Pressure Systems. It is ideal for applications such as dosing […]

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    • Aalborg Mass Flow Meter

      (optional)

      The Aalborg Mass Flow Meters are for use with Atlas Pressure Systems. They are ideal for applications such as understanding […]

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    • Atlas Syringe Pump

      (optional)

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    • Circulator and Fluid

      (optional)

      Circulator options from industry-leading manufacturer, Huber. A range of circulator accessories and oils for whatever your application are available.

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Support

These support articles may be helpful for this system

Contact us for more information

Do you have questions or need more details? Contact our expert team for more information on how the Atlas Potassium 3 Bar Pressure Reactor can meet your specific needs.

Contact us.