Pre-configured System
Atlas HD Reaction Calorimeter
An easy-to-use, high-performance calorimetry system. Using either Heat Flow Calorimetry (HFC) or Power Compensation Calorimetry (PCC), it can generate power and enthalpy graphs quickly and easily.
At a glance
The Atlas HD Reaction Calorimeter operates in either Heat Flow Calorimetry (HFC) or Power Compensation Calorimetry (PCC) mode. The system is designed for ease of use with the generation of power and enthalpy graphs made simple and quick.
In addition, the simple configuration of reaction temperatures, dosing quantities, and alarms, provides you with a safe and accurate reaction calorimetry system and offers great value for calorimetry chemists.
- Designed for ease of use
- Safe & accurate reaction calorimetry system
- Simple & quick power & enthalpy graph generation
1. HFC and PCC measurements
The system offers two modes; Heat Flow Calorimetry (HFC) or Power Compensation Calorimetry (PCC), allowing you to choose which mode is suitable for your process. HFC is generally used for reactions where the heater may have an effect on the chemistry since the dip in heater is not used during the reaction. HFC is also preferred when large exotherms are expected. PCC is used where quicker results are required, since no pre- and post-calibration is required. All important reaction parameters can be monitored in real-time using the Atlas HD Calorimeter.
2. Powerful automation
The Atlas PC Reaction Calorimetry Software offers truly easy reaction calorimetry operation. Configuration of parameters such as reaction temperature, dosing quantities, expected power level (e.g. moderate endotherm; strong exotherm), and alarms (with subsequent actions) are defined in an easy to use wizard. Everything is controlled automatically during the experiment including stabilization at desired reaction temperature, reagent addition and in the case of HFC, pre- and/or post-run calibration. No user intervention is required during the entire process.
3. Flexible
The Atlas HD Reaction Calorimeter is destined to be a very popular addition to your laboratory. Easy to set and configure, reaction calorimetry cannot be made simpler. A wide range of vacuum jacketed reactors from 100 mL to 2 L and the ability to perform HFC or PCC gives you choice. When there are no reaction calorimetry experiments to perform, the system will operate seamlessly as an automated jacketed reactor.
4. Quick and easy data analysis
The software automatically includes the calibration, compensates for the enthalpy of addition and deviations from isothermal conditions. Post experiment analysis is made easy by the Atlas Reporting Software featuring “single click” plotting of power and enthalpy.
Specifications
Vessel Volume Range | 50 mL, 100 mL, 250 mL, 500 mL, 1 L, 2 L (DN80), 1 L, 2 L, and 5 L (DN150) |
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Vessel Shapes | Torispherical, Conical, Round Bottom |
Vessel Profiles | Jacketed, Vacuum Jacketed |
Other Vessel Types | No (Round Bottom Flasks Available with Regular Atlas Base) |
Temperature Range | -90°C to 250°C (with suitable seal kit) |
Stirring Options | Scorpion Overhead Stirrer (up to 800rpm/11Ncm torque), High Speed Available, High Torque Available |
Automation | Yes – as standard |
Modes of Operation | Atlas HD Touch Screen Control, Atlas PC Software, Manual Operation |
Sensor Options | Temperature, pH, Pressure, Turbidity, In-situ FTIR, Other Sensors Available |
Pressure Range | Vacuum (50mbar) to 0.5 Bar, See Atlas 200 Bar Pressure Systems for High Pressure up to 200 Bar, See Atlas 3 Bar Pressure Systems for High Pressure up to 3 Bar |
Reaction Calorimetry | Heat Flow Calorimetry (HFC), Power Compensation Calorimetry (PCC) |
Reagent Addition and Sampling | Manual Dosing, Automated Dosing (Volumetric), Automated Dosing (Gravimetric), Sampling of Liquids, Full Gas Control, Atlas Syringe Pump Range |
Modules
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Base units
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Atlas HD Potassium
The Atlas HD Potassium is the base reactor system on which all Atlas HD systems are built, and can be […]
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Automation
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Atlas PC Software 1
Atlas Software 1 is an easy-to-use PC based application for control and analysis of experiments. Whole systems including stirrers, circulators, […]
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Atlas Reporting Software
The Atlas Reporting Software allows easy graphical analysis of log files generated by either the Base Unit, Atlas Software 1, […]
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Advanced Applications
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Atlas Calorimetry Upgrade Kit
The Atlas HD Calorimetry Upgrade Kit includes all the necessary parts to upgrade the Atlas HD Potassium base system to […]
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Circulation
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Circulator and Fluid
Circulator options from industry-leading manufacturer, Huber. A range of circulator accessories and oils for whatever your application are available.
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Dosing
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Atlas Syringe Pump
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Optional modules
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Atlas Syringe Pump
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Circulator and Fluid
Circulator options from industry-leading manufacturer, Huber. A range of circulator accessories and oils for whatever your application are available.
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Support
These support articles may be helpful for this system