Pre-configured System
Atlas HD Crystallization Reactor
Allows crystallization processes to be monitored and controlled, as well as performing sonocrystallization or sonomilling techniques.
Applications
This product is suitable for the following applications.
At a glance
The Atlas HD Crystallization Reactor allows turbidity to be monitored and modified by controlling temperature and/or additions of the vessel. Real-time data is displayed on the Atlas HD touchscreen and can be plotted using the software.
The proprietary ultrasound technology features a novel transducer-based design. It enablesof parameters such as particle size, shape, crystallinity, and polymorphism. Chemists have more reproducibility because of its design.
Monitor your reactions using the Atlas turbidity probe and node, and manage the process using the innovative SonoLab module for sonocrystallization or sonomilling techniques.
- Real-time data displayed & plotted on Atlas HD touchscreen
- Reproducible control over operations
Monitor your crystallization using the Atlas turbidity probe and node and control the process using the innovative SonoLab module to perform sonocrystallization or sonomilling techniques.
- Real-time data displayed & plotted on Atlas HD touch screen
- Reproducible control of crystallizations
Dimensions
| Smallest vessel: | 108cm H x 54cm W x 45cm D |
| Largest vessel: | 115cm H x 58cm W x 45cm D |
| Power: | 100-240 VAC, 50/60 Hz, 5A Fuse |
1. Controlled crystallization process using sonocrystallization techniques
Sonocrystallization is the application of high-intensity, low-frequency ultrasound, resulting in acoustic cavitation of the solution. Controlled cavitation enables extremely precise control of nucleation, a random process that is both random and difficult to regulate with conventional techniques. The reactor combines the powerful Atlas HD Potassium with a proprietary ultrasonic flow cell, generator, and recirculating pump, which can help manage nucleation and growth.
2. Exact control of cooling and anti-solvent crystallization
The reactor excels in managing both controlled cooling and anti-solvent crystallization. Using either the base unit or PC software, it employs sophisticated algorithms for precise temperature regulation, ensuring the process is maintained within the metastable zone. Anti-solvent crystallization is performed using the Atlas syringe pump, which offers precise dosing from 1 μL/min to 10 mL/min.
3. Unrivalled automation
The reactor has an intuitive touchscreen base, delivering unmatched capability to define and monitor conditions over a broad range of working volumes. The touch screen allows you to change parameters such as stirring, heating, and dosing in real-time and displays all data graphically. Further automation can be provided using PC software.
4. Narrow particle size distribution
Initiating nucleation using ultrasound offers reproducible crystallization. The crystal growth can also be controlled with ultrasonic energy providing a very uniform and narrow particle size distribution. Once crystals are formed, the system goes into sonomilling mode and varies the ultrasound’s intensity, allowing you to tailor the particle to your desired size. Third-party particle size monitors can also be integrated to ensure that the platform provides all you need to master your crystallization process.
What our customers say
Atlas HD reactor systems ensure each experiment is performed in exactly the same way every time.”
Specifications
| Vessel Volume Range | 50 mL, 100 mL, 250 mL, 500 mL, 1 L, 2 L (DN80), 1 L, 2 L, and 5 L (DN150) |
|---|---|
| Vessel Shapes | Torispherical, Conical, Round Bottom |
| Vessel Profiles | Jacketed, Vacuum Jacketed |
| Other Vessel Types | No (Round Bottom Flasks Available with Regular Atlas Base) |
| Temperature Range | -90°C to 250°C (with suitable seal kit) |
| Stirring Options | Scorpion Overhead Stirrer (up to 800rpm/11Ncm torque), High Speed Available, High Torque Available |
| Automation | Yes – using Atlas PC Software |
| Modes of Operation | Atlas HD Touch Screen Control, Atlas PC Software, Manual Operation |
| Sensor Options | Temperature, pH, Pressure, Turbidity, In-situ FTIR, Other Sensors Available |
| Pressure Range | Vacuum (50mbar) to 0.5 Bar, See Atlas 200 Bar Pressure Systems for High Pressure up to 200 Bar, See Atlas 3 Bar Pressure Systems for High Pressure up to 3 Bar |
| Reaction Calorimetry | Ability to Upgrade to Reaction Calorimetry, See Atlas HD Calorimeter |
| Reagent Addition and Sampling | Manual Dosing, Automated Dosing (Volumetric), Automated Dosing (Gravimetric), Sampling of Liquids, Full Gas Control, Atlas Syringe Pump Range |
Atlas HD Crystallization Reactor Key Features
The reactor is state-of-the-art and designed for advanced chemical processes. This customizable equipment features a 100L stainless steel tank, high borosilicate glass components, and a jacketed design for precise temperature control.
Material: High-quality stainless steel and PTFE, suitable for various chemical applications.
Design: Includes a motor, air filter, condenser, and insulation jacket for efficient operation.
Components: Equipped with a sophisticated controller for precise control, a chiller for temperature regulation, and various accessories for enhanced functionality.
Package: Comprehensive packages available, meeting different industry requirements.
Ease of Use: Easy-to-clean design with accessible parts and user-friendly interface.
Customization: Tailored options to meet specific needs, with additional accessories available.
Customer Support: Backed by extensive support from our company, including contact options for queries, reviews, and purchasing advice.
The reactor is designed to meet standard industry requirements and can be purchased as part of a package or as individual items, depending on your needs. Contact us to review features, components, and pricing to meet your specific laboratory requirements.
What we say
When performing crystallization reactions, the ability to quickly record data is critical. Atlas HD enables this at the touch of a button.”
Modules
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Base units
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Atlas HD Potassium
The Atlas HD Potassium is the base reactor system on which all Atlas HD systems are built, and can be […]
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Probes and Nodes
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Turbidity Probe and Node
Accurate measurement and monitoring of turbidity in partnership with the Atlas HD base. Turbidity Probe The Turbidity Probe can be […]
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Advanced Applications
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Prosonix Sonolab SL10 Sonocrystallizer (230V/110V)
The Prosonix Sonolab is a high-performance ultrasound module allowing full control of crystallization processes, for use with the Atlas HD […]
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Sonocrystallizer Accessories Pack
The Sonocrystallizer Accessories Pack contains a peristaltic pump, tubing, connectors, and valves for recycling the reactor contents through the Sonolab […]
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Circulation
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Circulator and Fluid
Circulator options from industry-leading manufacturer, Huber. A range of circulator accessories and oils for whatever your application are available.
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Dosing
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Atlas Syringe Pump
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Optional modules
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Atlas Syringe Pump
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Circulator and Fluid
Circulator options from industry-leading manufacturer, Huber. A range of circulator accessories and oils for whatever your application are available.
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Support
These support articles may be helpful for this system
Contact us today for more information
Do you have questions or need more details? Contact our expert team for more information on how the Atlas HD Crystallization Reactor can meet your specific needs.